Cryostat-600
Instrumentation
Cryostat-600 (KSC-TOPS-45)
Thermal Insulation/Structure Test Apparatus
Overview
NASA Kennedy Space Center seeks partners interested in the guarded two dimensional flat plate insulation test cryostat (Cryostat-600), a boil-off calorimeter comprised of a flat bottom test apparatus for measuring the absolute thermal performance of an insulation system. Various structural elements, struts, or supports can be placed through the insulation to evaluate two dimensional heating effects, especially on anisotropic materials, such as multilayer insulation (MLI) systems. Four threaded ports in the bottom of the calorimeter provide for attachment of the metal, plastic, or composite elements. The test chamber is guarded by a second cryogenic chamber to provide absolute measurement of the total heat load.
As the demands for energy-efficient systems on Earth and in space increase, the need for accurate thermal performance measurements of real-world insulation systems is increasing. The Cryostat-600 is capable of evaluating integrated insulation and structural systems, and it is adaptable to testing exotic, high performance systems or conventional building materials. The system is not limited to small temperature differences, and it can easily provide large temperature differences that are representative of the operational environment.
The Technology
The Cryostat-600 provides steady state thermal performance data, including the effective thermal conductivity and heat load, through insulation systems with or without structural elements. The cold boundary temperature can be varied at discrete points between 4 K and 80 K with warm boundary temperatures between approximately 250 K and 400 K. The vacuum level can be changed between 10E-7 torr and 10E3 torr, covering the full vacuum range and environments using different background gasses. Of greatest interest in this configuration is the high performance, high vacuum insulation systems that are not covered by existing ASTM test methods. The instrument has been proven through extensive testing of different multilayer insulation (MLI) systems, foams, and composites, including testing the effects of various structural elements.
Benefits
- Thermal measurement and testing of insulation materials and/or structural elements
- Proven through extensive testing of integrated insulation systems
- Direct heat measurement through boil-off calorimetry
- Cost effective and time efficient
- Testing over a wide range of environmental conditions: high vacuum to ambient pressure and from 4K to 400K
Applications
- Electrical power generation and transmission
- Refrigeration
- Medical imaging
- Food processing
- Electronics manufacturing
- Aerospace
- Construction materials
- Multiple energy-related industries and sectors
- Ground and air transportation (e.g., insulation used in hydrogen-based cars)
Similar Results
Cryostat-500
The Cryostat-500 provides laboratory measurement of the steady-state thermal transmission properties of thermal insulation systems under conditions below ambient temperature. Liquid nitrogen is used as a direct measure of the energy going through the test specimen. Thermal insulation systems may be composed of one or more materials that may be homogeneous or non-homogeneous at boundary conditions from 77 K to 373 K and in environments from high vacuum (10E-7 torr) to ambient pressure (10E+3 torr).
The Cryostat-500 provides a much wider range of thermal performance and covers the full range of environmental conditions for applications below ambient temperature. The instrument has been proven through extensive testing of foams, composite panels, multilayer insulation (MLI) systems, aerogel blankets, fiberglass, and many other types of materials. Both the quality and quantity of the thermal performance data for insulation materials and systems have increased even as the process and method has become more time efficient and cost effective. Further guidelines on the test method and equipment for the Cryostat-500 are given in ASTM C1774, Annex A3.
Cryostat-100
Cryostat-100 combines the best features of previous cryostats developed by NASA, while offering new features and conveniences. This unit can readily handle the full range of cryogenic-vacuum conditions over several orders of magnitude of heat flux. Guide rings, handling tools, and other design items make insulation change-out and test measurement verification highly reliable and efficient to operate. The new apparatus requires less ancillary equipment (it is not connected to storage tank, phase separator, subcooler, etc.) to operate properly. It is top-loading, which makes disassembly, change-out, and instrumentation hook-up much faster. The thermal stability is improved because of internal vapor plates, a single-tube system of filling and venting, bellows feed-throughs, Kevlar thread suspensions, and heavy-wall stainless-steel construction.
The cold mass of Cryostat-100 is 1m long, with a diameter of 168 mm. The test articles can therefore be of a corresponding length and diameter, with a nominal thickness of 25.4 mm. Shorter lengths are acceptable, and thicknesses may be from 0 mm to 50 mm. Tests are conducted from ambient pressure (760 torr) to high vacuum (below 110-4 torr) and at any vacuum pressure increment between these two extremes. The residual gas (and purge gas) is typically nitrogen but can be any purge gas, such as helium, argon, or carbon dioxide.
Typically, eight cold vacuum pressures are performed for each test series. The warm boundary temperature is approximately 293 K, and the cold boundary temperature is approximately 78 K. The delta temperature for the cryogenic testing is therefore approximately 215 K. A unique lift mechanism provides for change-out of the insulation test specimens. It also provides for maintenance and other operations in the most effective and time-efficient ways. The lift mechanism is also a key to the modularity of the overall system.
Cryostat-100
Cryostat-100 combines the best features of previous cryostats developed by NASA, while offering new features and conveniences. This unit can readily handle the full range of cryogenic-vacuum conditions over several orders of magnitude of heat flux. Guide rings, handling tools, and other design items make insulation change-out and test measurement verification highly reliable and efficient to operate. The new apparatus requires less ancillary equipment (it is not connected to storage tank, phase separator, subcooler, etc.) to operate properly. It is top-loading, which makes disassembly, change-out, and instrumentation hook-up much faster. The thermal stability is improved because of internal vapor plates, a single-tube system of filling and venting, bellows feed-throughs, Kevlar thread suspensions, and heavy-wall stainless-steel construction.
The cold mass of Cryostat-100 is 1m long, with a diameter of 168 mm. The test articles can therefore be of a corresponding length and diameter, with a nominal thickness of 25.4 mm. Shorter lengths are acceptable, and thicknesses may be from 0 mm to 50 mm. Tests are conducted from ambient pressure (760 torr) to high vacuum (below 110-4 torr) and at any vacuum pressure increment between these two extremes. The residual gas (and purge gas) is typically nitrogen but can be any purge gas, such as helium, argon, or carbon dioxide.
Typically, eight cold vacuum pressures are performed for each test series. The warm boundary temperature is approximately 293 K, and the cold boundary temperature is approximately 78 K. The delta temperature for the cryogenic testing is therefore approximately 215 K. A unique lift mechanism provides for change-out of the insulation test specimens. It also provides for maintenance and other operations in the most effective and time-efficient ways. The lift mechanism is also a key to the modularity of the overall system.
Macroflash (Cup Cryostat)
Advances in new polymers and composites along with growing industrial needs in below-ambient temperature applications have brought about the Macroflash development. Accurate thermal performance information, including effective thermal conductivity data, are needed under relevant end-use conditions. The Macroflash is a practical tool for basic testing of common materials or research evaluation of advanced materials/systems.
The Macroflash can test solids, foams, or powders that are homogeneous or layered in composition. Test specimens are typically 75mm in diameter and 6mm in thickness. The cold side is maintained by liquid nitrogen at 77 K while a heater disk maintains a steady warm-side temperature from ambient up to 373 K. The steady boiloff of the liquid nitrogen provides a direct measure of the heat energy transferred through the thickness of the test specimen. Nitrogen or other gas is supplied to the instrument to establish a stable, moisture-free, ambient pressure environment. Different compression loading levels can also be conveniently applied to the test specimen as needed for accurate, field-representative thermal performance data. The Macroflash is calibrated from approximately 10 mW/m-K to 800 mW/m-K using well-characterized materials.
Feedthrough for Severe Environments and Temperatures
Space and ground launch support related hardware often operate under extreme pressure, temperature, and corrosive conditions. When dealing with this type of equipment, it is frequently necessary to run wiring, tubes, or fibers through a barrier separating one process from another with one or both operating in extreme environments. Feedthroughs used to route the wiring, tubes, or fibers through these barriers must meet stringent sealing and leak tightness requirements.
This affordable NASA feedthrough meets or exceeds all sealing and leak requirements utilizing easy-to-assemble commercial-off-the-shelf hardware with no special tooling. The feedthrough is a fully reconfigurable design; however, it can also be produced as a permanent device. Thermal cycling and helium mass spectrometer leak testing under extreme conditions of full cryogenic temperatures and high vacuum have proven the sealing capability of this feedthrough with or without potting (epoxy fill) on the ends. Packing material disks used in the construction of the device can be replaced as needed for rebuilding a given feedthrough for another job or a different set of feeds if potting is not used for the original feedthrough build. (Potting on one or both sides of the sleeve provides double or triple leak sealing protection). Variable Compression Ratio (VCR) connectors were adapted for the pressure seal on the feedthrough; however, any commercial connector can be similarly adapted. The design can easily be scaled up to larger (2" diameter) and even very large (12" or more) sizes.



