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Without improvements in valve technologies, propellant and commodity losses will likely make long-duration space missions (e.g., to Mars) infeasible. Cryogenic valve leakage is often a result of misalignment and the seat seal not being perpendicular relative to the poppet. Conventional valve designs attempt to control alignment through tight tolerances across several mechanical interfaces, bolted or welded joints, machined part surfaces, etc. However, because such tight tolerances are difficult to maintain, leakage remains an issue. Traditional poppets are not self-aligning, and thus require large forces to “crush” the poppet and seat together in order to overcome misalignment and create a tight seal. In contrast, NASA’s poppet valve self-aligns the poppet to the valve seat to minimize leakage. Once the poppet and seat are precisely self-aligned, careful seat crush is provided. Owing to this unique design, the invention substantially reduces the energy required to make a tight seal – reducing size, weight, and power requirements relative to traditional valves. Testing at MSFC showed that NASA’s poppet reduces leakage rates of traditional aerospace cryogenic valves (~1000 SCIM) by three orders of magnitude, resulting in leakage rates suitable for long-duration space missions (~1 SCIM). NASA’s self-aligning poppet was originally targeted for aerospace cryogenic valve systems, especially for long-duration manned space missions – making the invention an attractive solution for aerospace valve vendors. The invention may also find use in the petrochemical or other industries that require sealing to prevent critical or hazardous chemicals from leaking into the environment. Generally, the invention may be suitable for any application requiring low-leak and/or long duration storage of expensive or limited resource commodities (e.g., cryogenic gases, natural gas, nuclear engines, etc).

The technology provides miniaturized techniques for extracting trace amounts of organic molecules (lipids) from natural samples. It operates as an autonomous, miniaturized fluidic system, integrating lab techniques for lipid analysis while minimizing reagent volumes and concentrating organics for analysis, thereby increasing signal-to-noise ratios by orders of magnitude. The non-aqueous fluidic system described herein for astrobiological and life-detection missions (either in situ or returned sample) is configured to extract lipid organics from regolith using (1) a fluidic sample processor made of materials compatible with organic solvents and (2) a machine-learning system to select processing steps and parameters to maximize lipid yield. A critical gap is bridged by integrating technologies into a system that replicates analytical lab procedures autonomously on a spaceflight instrument scale with fidelity to original lab techniques. Automated fluidic devices combine controlled handling of liquids with sequential operations and parallelization of replicate processes. By designing such systems to closely interface with both sample-delivery and analytical measurement systems, laboratory analyses are automated. The technology adapts best practice laboratory methods for lipid analysis, overcoming analytical challenges like low organic abundance, interference of minerals/salts, and degradation of origin-diagnostic molecular structures. The extraction and concentration techniques from rock/soil samples can be applied to any biomarkers by changing the solvent, temperature, and agitation.

The advent of additive manufacturing makes available new and innovative integrated thermal management systems, including integrating an oscillating Heat Pipe (OHP) into the leading edge of a hypersonic vehicle for rapid dissipation of large quantities of heat. OHPs have interconnected capillary channels filled with a working fluid that forms a train of liquid plugs and vapor bubbles to facilitate rapid heat transfer. Multiple additive manufacturing techniques may be used, including powder bed fusion, binder jetting, metal material extrusion, directed energy deposit, sheet lamination, ultrasonic, and electrochemical techniques. These high performance OHPs can be made with materials such as Refractory High Entropy Alloys (RHEAs) that can withstand high temperature applications. The structure of the OHP can be integrated into the constructed leading edge. The benefits include a heat transport capacity of 10 to 100 times greater than before. Integrated OHPs avoid the bends or welds in traditional heat pipes, especially at the locations where the highest thermal stresses might cause thermal-structural failure of a leading edge. Alternating the diameters of the OHP channels alleviate start-up issues typically found in liquid metal oscillating heat pipe designs in high temperature applications by aiding in the instigation of a circulating flow due to multiple forces acting upon the working fluid.

The innovative technology from Ames acts as a microfluidics switch array, using combinations of pressure and flow conditions to achieve specific logic states that determine the sequences of sample movement between microfluidic wells. This advancement will enable automation of complex laboratory techniques not possible with earlier microfluidics technologies that are designed to follow predetermined flow paths and well targets. This novel method also enables autonomous operations including changing the flow paths and targeting well configurations in situ based on measured data decision parameters. This microfluidic system can be reconfigured for use in various experimental applications, requiring only an adjustment of the programmed pressure sequencing, reducing the need for custom design and development for each new application. For example, this technology could provide the ability to selectively constrain or move biological specimens in the experimental wells, allowing evolutionary studies of model organisms in response to various stressors, evaluation of different growth conditions on biological production of antibodies or other small molecule therapeutics, among other potential applications. Likewise, this platform can be used to foster time-dependent, step-wise, chemical reactions, which could be used for novel chemical processes or in situ resource utilization.

This NASA Glenn innovation comprises a non-pneumatic, compliant tire utilizing shape memory alloys (mainly NiTi and its derivatives) as load bearing components. These shape memory alloys are capable of undergoing significant reversible strain (up to 10%), enabling the tire to withstand an order of magnitude more deformation than other non-pneumatic tires before undergoing permanent deformation. Commonly used elastic-plastic materials (e.g. spring steels, composites, etc.) can only be subjected to strains on the order of ~ 0.3-0.5% before yielding. Hence, the use of a NiTi shape memory alloy produces a superelastic tire that is virtually impervious to plastic deformation. In addition, the utilization of shape memory alloys provides enhanced control over the effective stiffness as a function of the deformation, providing increased design versatility. For instance, the Glenn Superelastic Tire can be made to soften with increased deflection, reducing the amount of energy transferred to the vehicle during high deformation events. In addition, the use of shape memory alloys in the form of radial stiffeners, as opposed to springs, provides even more load carrying potential and improved design flexibility. This type of compliant tire would allow for increased travel speeds in off-road applications.

For extremely high-temperature sealing applications, Glenn researchers have devised novel methods for fabricating single-crystal preloaders. NASA's high-temperature preloaders consist of investment cast or machined parts that are fabricated in various configurations from single crystal superalloys. Machined preloaders include a variety of spring configurations, compressed axially or radially, fabricated from single crystal slabs. Before machining, the slabs are carefully oriented in a special goniometer using x-diffraction techniques. This helps to maintain proper crystal orientation relative to the machined part and the applied loads. For more complex geometry components which cannot be easily and economically machined, an investment casting approach would be used. Complex preloader geometries include wire coil springs of various configurations. These single crystal preloaders would be designed with the appropriate stiffness for the intended thermal barrier/seal application and placed underneath, or integrated within, the seal/barrier. At extrememly high temperature, the preload device keeps the seal/barrier mated against the opposing surface as the gap between the two surfaces changes, maintaining contact between surfaces and preventing convective heat transfer.

Glenn's revolutionary SMARS device is fabricated from nickel-titanium-halfnium (NiTiHf), nickel-titanium-zirconium compositions, or a combination. These compositions contain a secondary, nanometer-sized precipitate phase, which is produced through processes of compositional control and ageing heat treatments. Glenn's novel materials and processes have yielded a SMA composition that produces much higher stresses than other SMAs on the commercial market. The SMARS device is composed of 1) SMA material as the actuating member; 2) a casing heater placed around the SMA member; 3) a DC or AC power source to provide current through the heater; 4) pointed tips for acute penetration into rock formations; and 5) a hand-press to reset the SMA element after each use. In the rock-splitting process, a hole equal to the diameter of the SMA element is drilled in the portion of the rock where the fracture is desired. Next, the pre-compressed SMA is inserted into the hole, and AC or DC current is applied to energize the devices heaters. Once the heater achieves the critical transformation temperature, the SMA will begin to expand within seconds. Since its expansion is constrained by the rock walls, the SMA will eventually exert up to 1500 MPa of stress, splitting the rock apart. When the current is removed and the heater cools, the SMA material returns to its pre-compressed state. At this point, the material can be recovered, so the process is repeatable after reshaping. The SMA actuating members were also designed to achieve displacement greater than the materials strain output. Glenns SMARS device provides high-powered rock fracturing that is controllable, reliable, and comparatively simple without the use of explosives, hydraulics, or chemicals.

Approximately 50 inches in diameter, Glenn's unique sealing system consists of multiple elements installed in a recessed rectangular sealing groove. The main sealing function is provided by an elastomer element (e.g., silicone) comprising one or more sealing wall(s) connected by a web. The wall(s) extend above the top of the sealing groove so they are compressed by the opposing mating surface during the sealing process. The retractable shroud element is installed between the wall(s), with its base resting atop the web of the sealing element. The shroud is typically composed of an elastomer material to allow for flexibility (which is essential to retraction), but it can also be made from thin metal or plastic materials. When the seal is no longer in use, a pair of V-shaped shroud "arms" extend upward from the base of the seal to cover the wall(s). A thin metal retainer is installed on top of the shroud, and fasteners pass through holes in the retainer, shroud, and sealing elements to secure the system to the base of the sealing groove. Metal washers are installed in these holes to provide a load path between the metal retainer and the surface of the sealing groove. The system can seal against either a flat metal surface or another seal of the same design. This sealing system has been designed to accommodate multiple sealing cycles and has exhibited extremely low leak rates, making it an attractive solution within a variety of industries from aerospace to agriculture.

For the very first time, NASA Glenn has successfully produced large quantities of high-grade ball bearings that are less than 0.25" in diameter thanks to the development of a new alloy made of 57.6% Ni, 39.2% Ti and 3.2% Hf. Smaller, shockproof balls improve load capability in conventional steel races, aircraft control surface joints, actuator gearboxes, and more. The production of standard NiTi alloy ball bearings that are smaller than 0.375" in diameter has proven challenging for multiple reasons, the primary being that small parts made from NiTi alloys cool excessively before they can be quenched (an important step in attaining high hardness). NiTi-Hf alloy, on the other hand, does not require such high-rate quenching to achieve high hardness. Consequently, the production of small, extremely durable NiTi ball bearings is now a reality. The powder metallurgy process by which these high-quality NiTi-Hf ball bearings are manufactured combines many new techniques with several existing ones. First, a high-purity NiTi-Hf powder is created through an atomization process and transformed into long, cylindrical rods through hot isostatic pressing. The rods are then cut into cylinders and machined into spheres somewhat larger than the desired finished ball size. Finally, the spheres are hardened through heat treatment and polished until the desired finished size diameter and surface finish (typically 1 micro-inch root mean square roughness) is achieved. The result is a non-corrosive, very hard, highly elastic yet remarkably strong ball bearing with unbridled potential.